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SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.分析儀,就選上海禹重實(shí)業(yè)有限公司,用戶的信賴之選,歡迎新老客戶來(lái)電!化學(xué)分析儀廠家直銷(xiāo)
Procedure–Powder/ChipSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.LoginaminimumofthreeBlankreps.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Inserta***NickelCapsule(leavecapsuleopen)intotheopenportattopofloadinghead.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.江蘇氧氮?dú)浞治鰞x怎么樣分析儀,就選上海禹重實(shí)業(yè)有限公司,用戶的信賴之選,有需求可以來(lái)電咨詢!
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.AnalyzeSamples.LoginSamplewiththeappropriatenumberofreps.Weighapproximately***gramsofappropriatelypreparedsampleintoa***NickelCapsule,entermassandsampleidentificationintoappropriaterepfields.Ifapplicable,placethenickelcapsuleintheappropriateautoloaderposition.Repeatsteps3cthrough3iforsampleanalysis.
Procedure–Powder/ChipSamplesDeterminetheinstrumentblank.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.LoginaminimumofthreeStandardreps.Weighapproximately***gramsofacalibration/driftstandardintoa***NickelCapsule;enterthemassandstandardidentificationintoappropriaterepfields.Ifapplicable,placethenickelcapsuleintheappropriateautoloaderposition.Note:LECOReferenceMateria***onotrequirepreparation.Seepreparationstatementonthereferencematerialcertificate.SolidStandardsmaybeusedtocalibratewhenchiporpowderstandardsarenotavailable.分析儀,就選上海禹重實(shí)業(yè)有限公司,用戶的信賴之選。
ONH836系列:氧氮?dú)浞治鰞x(熔融法)力可ONH836系列儀器采用惰性熔融法,提供各種無(wú)機(jī)材料、鋼鐵、有色金屬、硬質(zhì)合金、陶瓷材料中寬范圍的氧氮?dú)渫瑫r(shí)分析。ONH836系列儀器通過(guò)***采納客戶的反饋意見(jiàn)和創(chuàng)新設(shè)計(jì),力可***儀器采用觸摸屏技術(shù)和在線軟件平臺(tái),增強(qiáng)了儀器的可操作性、降低了分析成本、節(jié)省實(shí)驗(yàn)室桌面空間。用戶友好界面的Cornerstone?軟件力可的Cornerstone氧氮氧分析軟件采用觸摸屏界面使用戶可完整的達(dá)到分析控制、方法設(shè)定、在線診斷、數(shù)據(jù)報(bào)告。Cornerstone氧氮氧分析軟件允許用戶在單一分析界面中完成日常的所有工作,快速而且簡(jiǎn)單易用。力可創(chuàng)新的批次和重復(fù)樣品數(shù)據(jù)分組功能極大簡(jiǎn)化了樣品結(jié)果輸出和結(jié)果標(biāo)準(zhǔn)偏差的自動(dòng)計(jì)算,減少了繁瑣的額外數(shù)據(jù)處理。分析儀,就選上海禹重實(shí)業(yè)有限公司,讓您滿意,歡迎新老客戶來(lái)電!天津進(jìn)口力可氧氮?dú)浞治鰞x
分析儀,就選上海禹重實(shí)業(yè)有限公司,用戶的信賴之選,有需要可以聯(lián)系我司哦!化學(xué)分析儀廠家直銷(xiāo)
Instrumentcalibration/driftcorrectionf.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.g.Firmlyplaceagraphitecrucibleonthelowerelectrodetip.h.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.i.Repeatsteps3bthrough3haminimumofthreetimesforeachcalibration/driftstandardused..Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.化學(xué)分析儀廠家直銷(xiāo)